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16.2 What is the effect of oven drying on volumetric glassware? (Chemistry)




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This article is from the Chemistry FAQ, by Bruce Hamilton B.Hamilton@irl.cri.nz with numerous contributions by others.

16.2 What is the effect of oven drying on volumetric glassware? (Chemistry)

Many older laboratory texts insist that volumetric glassware should not
be oven dried because of the danger of irreversible and unpredictable
volume changes. However most modern laboratory glassware is now made of
Pyrex, and work by D.R.Burfield has demonstrated that low temperature
drying does not significantly affect the calibration of volumetric
glassware [10]. He demonstrated that exposing volumetric flasks and
pipettes to 320C, either continuously or thermally cycled, resulted in no
significant detectable change to the calibration. He concluded that
"oven temperatures in the range of 110-150C should provide efficient drying
of glassware with no risk of discernible volume changes, even after
prolonged use, providing that Pyrex glass is the material of construction".

 

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